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Solvent-resistant nanofiltration for product purification and catalyst recovery in Click chemistry reactions

Angels Cano-Odena, Pieter Vandezande, David Fournier UGent, Wim Van Camp UGent, Filip Du Prez UGent and Ivo Vankelecom (2010) CHEMISTRY-A EUROPEAN JOURNAL. 16(3). p.1061-1067
abstract
The quickly developing field of "click" chemistry Would undoubtedly benefit from the availability of an easy and efficient technology for product purification to reduce the potential health risks associated with the presence of copper in the final product. Therefore. solvent-resistant nanofiltration (SRNF) membranes have been developed to selectively separate "clicked" polymers from the copper catalyst and solvent. By using these solvent-stable cross-linked polyimide membranes in diafiltration, up to 98% of the initially present copper could be removed through the membrane together with the DMF solvent, the polymer product being almost completely retained. This paper also presents the first SRNF application in which the catalyst permeates through the membrane and the reaction product is retained.
Please use this url to cite or link to this publication:
author
organization
year
type
journalArticle (original)
publication status
published
subject
keyword
EFFICIENT, POLYMERS, DENDRIMERS, click chemistry, CYCLOADDITIONS, product purification, copper polymers, SEPARATION, solvent-resistant nanofiltration, KeyWords Plus: TRANSFER RADICAL POLYMERIZATION, HOMOGENEOUS CATALYSIS, IONIC LIQUID, MEMBRANES, COPPER-FREE
journal title
CHEMISTRY-A EUROPEAN JOURNAL
Chem. Eur. J.
volume
16
issue
3
pages
1061 - 1067
Web of Science type
Article
Web of Science id
000274615700041
JCR category
CHEMISTRY, MULTIDISCIPLINARY
JCR impact factor
5.476 (2010)
JCR rank
18/142 (2010)
JCR quartile
1 (2010)
ISSN
0947-6539
DOI
10.1002/chem.200901659
language
English
UGent publication?
yes
classification
A1
copyright statement
I have transferred the copyright for this publication to the publisher
id
941924
handle
http://hdl.handle.net/1854/LU-941924
date created
2010-05-04 13:25:29
date last changed
2010-06-15 14:59:22
@article{941924,
  abstract     = {The quickly developing field of {\textacutedbl}click{\textacutedbl} chemistry Would undoubtedly benefit from the availability of an easy and efficient technology for product purification to reduce the potential health risks associated with the presence of copper in the final product. Therefore. solvent-resistant nanofiltration (SRNF) membranes have been developed to selectively separate {\textacutedbl}clicked{\textacutedbl} polymers from the copper catalyst and solvent. By using these solvent-stable cross-linked polyimide membranes in diafiltration, up to 98\% of the initially present copper could be removed through the membrane together with the DMF solvent, the polymer product being almost completely retained. This paper also presents the first SRNF application in which the catalyst permeates through the membrane and the reaction product is retained.},
  author       = {Cano-Odena, Angels  and Vandezande, Pieter and Fournier, David and Van Camp, Wim and Du Prez, Filip and Vankelecom, Ivo},
  issn         = {0947-6539},
  journal      = {CHEMISTRY-A EUROPEAN JOURNAL},
  keyword      = {EFFICIENT,POLYMERS,DENDRIMERS,click chemistry,CYCLOADDITIONS,product purification,copper polymers,SEPARATION,solvent-resistant nanofiltration,KeyWords Plus: TRANSFER RADICAL POLYMERIZATION,HOMOGENEOUS CATALYSIS,IONIC LIQUID,MEMBRANES,COPPER-FREE},
  language     = {eng},
  number       = {3},
  pages        = {1061--1067},
  title        = {Solvent-resistant nanofiltration for product purification and catalyst recovery in Click chemistry reactions},
  url          = {http://dx.doi.org/10.1002/chem.200901659},
  volume       = {16},
  year         = {2010},
}

Chicago
Cano-Odena, Angels , Pieter Vandezande, David Fournier, Wim Van Camp, Filip Du Prez, and Ivo Vankelecom. 2010. “Solvent-resistant Nanofiltration for Product Purification and Catalyst Recovery in Click Chemistry Reactions.” Chemistry-a European Journal 16 (3): 1061–1067.
APA
Cano-Odena, Angels , Vandezande, P., Fournier, D., Van Camp, W., Du Prez, F., & Vankelecom, I. (2010). Solvent-resistant nanofiltration for product purification and catalyst recovery in Click chemistry reactions. CHEMISTRY-A EUROPEAN JOURNAL, 16(3), 1061–1067.
Vancouver
1.
Cano-Odena A, Vandezande P, Fournier D, Van Camp W, Du Prez F, Vankelecom I. Solvent-resistant nanofiltration for product purification and catalyst recovery in Click chemistry reactions. CHEMISTRY-A EUROPEAN JOURNAL. 2010;16(3):1061–7.
MLA
Cano-Odena, Angels , Pieter Vandezande, David Fournier, et al. “Solvent-resistant Nanofiltration for Product Purification and Catalyst Recovery in Click Chemistry Reactions.” CHEMISTRY-A EUROPEAN JOURNAL 16.3 (2010): 1061–1067. Print.