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A general protocol for the synthesis of Pt-NHC (NHC = N-heterocyclic carbene) hydrosilylation catalysts

Benon Maliszewski (UGent) , Nikolaos Tzouras (UGent) , Sébastien Guillet (UGent) , Marina Saab (UGent) , Marek Beliš (UGent) , Kristof Van Hecke (UGent) , Fady Nahra (UGent) and Steven Nolan (UGent)
(2020) DALTON TRANSACTIONS. 49(41). p.14673-14679
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Abstract
A general, user-friendly synthetic route to [Pt(NHC)(L)Cl-2] and [Pt(NHC)(dvtms)] (L = DMS, Py; DMS = dimethyl sulfide, dvtms = divinyltetramethylsiloxane, Py = pyridine) complexes has been developed. The procedure is applicable to a wide range of ligands and enables facile synthetic access to key Pt(0)- and Pt (II)-NHC complexes used in hydrosilylation catalysis.
Keywords
STRUCTURAL-CHARACTERIZATION, COMPLEXES SYNTHESIS, ALKYNES, BEARING, ROUTES, BR, CL

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MLA
Maliszewski, Benon, et al. “A General Protocol for the Synthesis of Pt-NHC (NHC = N-Heterocyclic Carbene) Hydrosilylation Catalysts.” DALTON TRANSACTIONS, vol. 49, no. 41, 2020, pp. 14673–79, doi:10.1039/d0dt03480k.
APA
Maliszewski, B., Tzouras, N., Guillet, S., Saab, M., Beliš, M., Van Hecke, K., … Nolan, S. (2020). A general protocol for the synthesis of Pt-NHC (NHC = N-heterocyclic carbene) hydrosilylation catalysts. DALTON TRANSACTIONS, 49(41), 14673–14679. https://doi.org/10.1039/d0dt03480k
Chicago author-date
Maliszewski, Benon, Nikolaos Tzouras, Sébastien Guillet, Marina Saab, Marek Beliš, Kristof Van Hecke, Fady Nahra, and Steven Nolan. 2020. “A General Protocol for the Synthesis of Pt-NHC (NHC = N-Heterocyclic Carbene) Hydrosilylation Catalysts.” DALTON TRANSACTIONS 49 (41): 14673–79. https://doi.org/10.1039/d0dt03480k.
Chicago author-date (all authors)
Maliszewski, Benon, Nikolaos Tzouras, Sébastien Guillet, Marina Saab, Marek Beliš, Kristof Van Hecke, Fady Nahra, and Steven Nolan. 2020. “A General Protocol for the Synthesis of Pt-NHC (NHC = N-Heterocyclic Carbene) Hydrosilylation Catalysts.” DALTON TRANSACTIONS 49 (41): 14673–14679. doi:10.1039/d0dt03480k.
Vancouver
1.
Maliszewski B, Tzouras N, Guillet S, Saab M, Beliš M, Van Hecke K, et al. A general protocol for the synthesis of Pt-NHC (NHC = N-heterocyclic carbene) hydrosilylation catalysts. DALTON TRANSACTIONS. 2020;49(41):14673–9.
IEEE
[1]
B. Maliszewski et al., “A general protocol for the synthesis of Pt-NHC (NHC = N-heterocyclic carbene) hydrosilylation catalysts,” DALTON TRANSACTIONS, vol. 49, no. 41, pp. 14673–14679, 2020.
@article{8694703,
  abstract     = {A general, user-friendly synthetic route to [Pt(NHC)(L)Cl-2] and [Pt(NHC)(dvtms)] (L = DMS, Py; DMS = dimethyl sulfide, dvtms = divinyltetramethylsiloxane, Py = pyridine) complexes has been developed. The procedure is applicable to a wide range of ligands and enables facile synthetic access to key Pt(0)- and Pt (II)-NHC complexes used in hydrosilylation catalysis.},
  author       = {Maliszewski, Benon and Tzouras, Nikolaos and Guillet, Sébastien and Saab, Marina and Beliš, Marek and Van Hecke, Kristof and Nahra, Fady and Nolan, Steven},
  issn         = {1477-9226},
  journal      = {DALTON TRANSACTIONS},
  keywords     = {STRUCTURAL-CHARACTERIZATION,COMPLEXES SYNTHESIS,ALKYNES,BEARING,ROUTES,BR,CL},
  language     = {eng},
  number       = {41},
  pages        = {14673--14679},
  title        = {A general protocol for the synthesis of Pt-NHC (NHC = N-heterocyclic carbene) hydrosilylation catalysts},
  url          = {http://dx.doi.org/10.1039/d0dt03480k},
  volume       = {49},
  year         = {2020},
}

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