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Composite materials based on Ag nanoparticles in situ synthesized on the vaterite porous matrices

Roman Kamyshinsky, Irina Marchenko, Bogdan Parakhonskiy (UGent) , Alexey Yashchenok, Yury Chesnokov, Alexey Mikhutkin, Dmitry Gorin, Alexander Vasiliev and Tatiana Bukreeva
(2018) NANOTECHNOLOGY. 30(3).
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Abstract
We have designed sensors based on Ag nanoparticles synthesized in situ on the vaterite beads. In this article we demonstrate an approach to produce size controllable spherical and elliptical vaterite particles and discuss time-dependent in situ Ag nanoparticles synthesis and its potential effect on surface-enhanced Raman scattering. The time dependent silver reduction synthesis in inorganic porous particles allows to regulate the number and size of Ag nanoparticles. It is shown that the irregular surface and high porosity of vaterite particles and large amount (surface filling factor) of the Ag nanoparticles are the critical parameters to increase the SERS signal to 104 times. Such inorganic composites have a huge potential in medical applications; soon they provide an opportunity to study intracellular processes in vivo. The detailed characterization of the microstructure of these composites was studied by scanning and transmission electron microscopy, including 3D visualization and energy dispersive x-ray microanalysis.
Keywords
vaterite, silver nanoparticles, SERS, Raman, colloids, calcium carbonate, CALCIUM-CARBONATE PARTICLES, ENHANCED RAMAN-SCATTERING, SILVER NANOPARTICLES, POLYELECTROLYTE MICROCAPSULES, METAL NANOPARTICLES, GOLD NANOPARTICLES, DRUG-DELIVERY, SIZE, CAPSULES, RELEASE

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Citation

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MLA
Kamyshinsky, Roman, et al. “Composite Materials Based on Ag Nanoparticles in Situ Synthesized on the Vaterite Porous Matrices.” NANOTECHNOLOGY, vol. 30, no. 3, 2018, doi:10.1088/1361-6528/aaea38.
APA
Kamyshinsky, R., Marchenko, I., Parakhonskiy, B., Yashchenok, A., Chesnokov, Y., Mikhutkin, A., … Bukreeva, T. (2018). Composite materials based on Ag nanoparticles in situ synthesized on the vaterite porous matrices. NANOTECHNOLOGY, 30(3). https://doi.org/10.1088/1361-6528/aaea38
Chicago author-date
Kamyshinsky, Roman, Irina Marchenko, Bogdan Parakhonskiy, Alexey Yashchenok, Yury Chesnokov, Alexey Mikhutkin, Dmitry Gorin, Alexander Vasiliev, and Tatiana Bukreeva. 2018. “Composite Materials Based on Ag Nanoparticles in Situ Synthesized on the Vaterite Porous Matrices.” NANOTECHNOLOGY 30 (3). https://doi.org/10.1088/1361-6528/aaea38.
Chicago author-date (all authors)
Kamyshinsky, Roman, Irina Marchenko, Bogdan Parakhonskiy, Alexey Yashchenok, Yury Chesnokov, Alexey Mikhutkin, Dmitry Gorin, Alexander Vasiliev, and Tatiana Bukreeva. 2018. “Composite Materials Based on Ag Nanoparticles in Situ Synthesized on the Vaterite Porous Matrices.” NANOTECHNOLOGY 30 (3). doi:10.1088/1361-6528/aaea38.
Vancouver
1.
Kamyshinsky R, Marchenko I, Parakhonskiy B, Yashchenok A, Chesnokov Y, Mikhutkin A, et al. Composite materials based on Ag nanoparticles in situ synthesized on the vaterite porous matrices. NANOTECHNOLOGY. 2018;30(3).
IEEE
[1]
R. Kamyshinsky et al., “Composite materials based on Ag nanoparticles in situ synthesized on the vaterite porous matrices,” NANOTECHNOLOGY, vol. 30, no. 3, 2018.
@article{8610415,
  abstract     = {{We have designed sensors based on Ag nanoparticles synthesized in situ on the vaterite beads. In this article we demonstrate an approach to produce size controllable spherical and elliptical vaterite particles and discuss time-dependent in situ Ag nanoparticles synthesis and its potential effect on surface-enhanced Raman scattering. The time dependent silver reduction synthesis in inorganic porous particles allows to regulate the number and size of Ag nanoparticles. It is shown that the irregular surface and high porosity of vaterite particles and large amount (surface filling factor) of the Ag nanoparticles are the critical parameters to increase the SERS signal to 104 times. Such inorganic composites have a huge potential in medical applications; soon they provide an opportunity to study intracellular processes in vivo. The detailed characterization of the microstructure of these composites was studied by scanning and transmission electron microscopy, including 3D visualization and energy dispersive x-ray microanalysis.}},
  articleno    = {{035603}},
  author       = {{Kamyshinsky, Roman and Marchenko, Irina and Parakhonskiy, Bogdan and Yashchenok, Alexey and Chesnokov, Yury and Mikhutkin, Alexey and Gorin, Dmitry and Vasiliev, Alexander and Bukreeva, Tatiana}},
  issn         = {{0957-4484}},
  journal      = {{NANOTECHNOLOGY}},
  keywords     = {{vaterite,silver nanoparticles,SERS,Raman,colloids,calcium carbonate,CALCIUM-CARBONATE PARTICLES,ENHANCED RAMAN-SCATTERING,SILVER NANOPARTICLES,POLYELECTROLYTE MICROCAPSULES,METAL NANOPARTICLES,GOLD NANOPARTICLES,DRUG-DELIVERY,SIZE,CAPSULES,RELEASE}},
  language     = {{eng}},
  number       = {{3}},
  pages        = {{10}},
  title        = {{Composite materials based on Ag nanoparticles in situ synthesized on the vaterite porous matrices}},
  url          = {{http://doi.org/10.1088/1361-6528/aaea38}},
  volume       = {{30}},
  year         = {{2018}},
}
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