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Polycapillary optics based confocal micro X-ray fluorescence and X-ray absorption spectroscopy setup at the European Synchrotron Radiation Facility Collaborative Research Group Dutch-Belgian Beamline, BM26A

(2018) ANALYTICAL CHEMISTRY. 90(3). p.2389-2394
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Abstract
A novel plug-and-play setup based on polycapillary X-ray optics enables three-dimensional (3D) confocal X-ray fluorescence (XRF) and X-ray absorption spectroscopy down to 8 X 8 X 11 mu m(3) (17 keV) at the European Synchrotron Radiation Facility Collaborative Research Group Dutch-Belgian Beamline, BM26A. A complete description and analytical characterization is presented, together with two recently performed experimental cases. In Deep Earth diamond SAo Luiz-Frankfurt am Main 16, an olivine-rich inclusion was mapped with full 3D XRF elemental imaging. The preliminary tests on Iron Gall ink contained in an historical document, a letter from the court of King Philip II of Spain, reveal both the delicate nature of Iron Gall ink and the lack of Fe-Ni chemical bonding.
Keywords
IRON-GALL INK, TRANSITION ZONE, XANES, QUANTIFICATION, SPECIATION, SPECTRA, DIAMOND, MANTLE, PAPER

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Citation

Please use this url to cite or link to this publication:

Chicago
Bauters, Stephen, Pieter Tack, Jennifer Helen Rudloff-Grund, Dipanjan Banerjee, Alessandro Longo, Bart Vekemans, Wim Bras, Frank E Brenker, Roelof van Silfhout, and Laszlo Vincze. 2018. “Polycapillary Optics Based Confocal Micro X-ray Fluorescence and X-ray Absorption Spectroscopy Setup at the European Synchrotron Radiation Facility Collaborative Research Group Dutch-Belgian Beamline, BM26A.” Analytical Chemistry 90 (3): 2389–2394.
APA
Bauters, S., Tack, P., Rudloff-Grund, J. H., Banerjee, D., Longo, A., Vekemans, B., Bras, W., et al. (2018). Polycapillary optics based confocal micro X-ray fluorescence and X-ray absorption spectroscopy setup at the European Synchrotron Radiation Facility Collaborative Research Group Dutch-Belgian Beamline, BM26A. ANALYTICAL CHEMISTRY, 90(3), 2389–2394.
Vancouver
1.
Bauters S, Tack P, Rudloff-Grund JH, Banerjee D, Longo A, Vekemans B, et al. Polycapillary optics based confocal micro X-ray fluorescence and X-ray absorption spectroscopy setup at the European Synchrotron Radiation Facility Collaborative Research Group Dutch-Belgian Beamline, BM26A. ANALYTICAL CHEMISTRY. 2018;90(3):2389–94.
MLA
Bauters, Stephen et al. “Polycapillary Optics Based Confocal Micro X-ray Fluorescence and X-ray Absorption Spectroscopy Setup at the European Synchrotron Radiation Facility Collaborative Research Group Dutch-Belgian Beamline, BM26A.” ANALYTICAL CHEMISTRY 90.3 (2018): 2389–2394. Print.
@article{8544743,
  abstract     = {A novel plug-and-play setup based on polycapillary X-ray optics enables three-dimensional (3D) confocal X-ray fluorescence (XRF) and X-ray absorption spectroscopy down to 8 X 8 X 11 mu m(3) (17 keV) at the European Synchrotron Radiation Facility Collaborative Research Group Dutch-Belgian Beamline, BM26A. A complete description and analytical characterization is presented, together with two recently performed experimental cases. In Deep Earth diamond SAo Luiz-Frankfurt am Main 16, an olivine-rich inclusion was mapped with full 3D XRF elemental imaging. The preliminary tests on Iron Gall ink contained in an historical document, a letter from the court of King Philip II of Spain, reveal both the delicate nature of Iron Gall ink and the lack of Fe-Ni chemical bonding.},
  author       = {Bauters, Stephen and Tack, Pieter and Rudloff-Grund, Jennifer Helen and Banerjee, Dipanjan and Longo, Alessandro and Vekemans, Bart and Bras, Wim and Brenker, Frank E and van Silfhout, Roelof and Vincze, Laszlo},
  issn         = {0003-2700},
  journal      = {ANALYTICAL CHEMISTRY},
  keywords     = {IRON-GALL INK,TRANSITION ZONE,XANES,QUANTIFICATION,SPECIATION,SPECTRA,DIAMOND,MANTLE,PAPER},
  language     = {eng},
  number       = {3},
  pages        = {2389--2394},
  title        = {Polycapillary optics based confocal micro X-ray fluorescence and X-ray absorption spectroscopy setup at the European Synchrotron Radiation Facility Collaborative Research Group Dutch-Belgian Beamline, BM26A},
  url          = {http://dx.doi.org/10.1021/acs.analchem.7b05110},
  volume       = {90},
  year         = {2018},
}

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