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The analysis of European lacquer : optimization of thermochemolysis temperature of natural resins

Louise Decq UGent, Frederic Lynen UGent, Michael Schilling, Wim Fremout, Vincent Cattersel, Delphine Steyaert, Charles Indekeu, Emile Van Binnebeke and Steven Saverwyns (2016) APPLIED PHYSICS A-MATERIALS SCIENCE & PROCESSING. 122(12).
abstract
In order to optimize chromatographic analysis of European lacquer, thermochemolysis temperature was evaluated for the analysis of natural resins. Five main ingredients of lacquer were studied: sandarac, mastic, colophony, Manila copal and Congo copal. For each, five temperature programs were tested: four fixed temperatures (350, 480, 550, 650 degrees C) and one ultrafast thermal desorption (UFD), in which the temperature rises from 350 to 660 degrees C in 1 min. In total, the integrated signals of 27 molecules, partially characterizing the five resins, were monitored to compare the different methods. A compromise between detection of compounds released at low temperatures and compounds formed at high temperatures was searched. 650 degrees C is too high for both groups, 350 degrees C is best for the first, and 550 degrees C for the second. Fixed temperatures of 480 degrees C or UFD proved to be a consensus in order to detect most marker molecules. UFD was slightly better for the molecules released at low temperatures, while 480 degrees C showed best compounds formed at high temperatures.
Please use this url to cite or link to this publication:
author
organization
year
type
journalArticle (original)
publication status
published
subject
keyword
GAS CHROMATOGRAPHY/MASS SPECTROMETRY, AGING BEHAVIOR, DAEMONOROPS-DRACO, MASS-SPECTROMETRY, SICCATIVE OILS, ART MATERIALS, MANILA COPAL, PYROLYSIS-GC, GEOSPHERE, FATE
journal title
APPLIED PHYSICS A-MATERIALS SCIENCE & PROCESSING
Appl. Phys. A-Mater. Sci. Process.
volume
122
issue
12
article number
1007
pages
8 pages
Web of Science type
Article
Web of Science id
000391422900015
JCR category
PHYSICS, APPLIED
JCR impact factor
1.455 (2016)
JCR rank
93/147 (2016)
JCR quartile
3 (2016)
ISSN
0947-8396
1432-0630
DOI
10.1007/s00339-016-0550-5
language
English
UGent publication?
yes
classification
A1
copyright statement
I have transferred the copyright for this publication to the publisher
id
8516626
handle
http://hdl.handle.net/1854/LU-8516626
date created
2017-03-31 12:49:19
date last changed
2017-05-29 12:56:35
@article{8516626,
  abstract     = {In order to optimize chromatographic analysis of European lacquer, thermochemolysis temperature was evaluated for the analysis of natural resins. Five main ingredients of lacquer were studied: sandarac, mastic, colophony, Manila copal and Congo copal. For each, five temperature programs were tested: four fixed temperatures (350, 480, 550, 650 degrees C) and one ultrafast thermal desorption (UFD), in which the temperature rises from 350 to 660 degrees C in 1 min. In total, the integrated signals of 27 molecules, partially characterizing the five resins, were monitored to compare the different methods. A compromise between detection of compounds released at low temperatures and compounds formed at high temperatures was searched. 650 degrees C is too high for both groups, 350 degrees C is best for the first, and 550 degrees C for the second. Fixed temperatures of 480 degrees C or UFD proved to be a consensus in order to detect most marker molecules. UFD was slightly better for the molecules released at low temperatures, while 480 degrees C showed best compounds formed at high temperatures.},
  articleno    = {1007},
  author       = {Decq, Louise and Lynen, Frederic and Schilling, Michael and Fremout, Wim and Cattersel, Vincent and Steyaert, Delphine and Indekeu, Charles and Van Binnebeke, Emile and Saverwyns, Steven},
  issn         = {0947-8396},
  journal      = {APPLIED PHYSICS A-MATERIALS SCIENCE \& PROCESSING},
  keyword      = {GAS CHROMATOGRAPHY/MASS SPECTROMETRY,AGING BEHAVIOR,DAEMONOROPS-DRACO,MASS-SPECTROMETRY,SICCATIVE OILS,ART MATERIALS,MANILA COPAL,PYROLYSIS-GC,GEOSPHERE,FATE},
  language     = {eng},
  number       = {12},
  pages        = {8},
  title        = {The analysis of European lacquer : optimization of thermochemolysis temperature of natural resins},
  url          = {http://dx.doi.org/10.1007/s00339-016-0550-5},
  volume       = {122},
  year         = {2016},
}

Chicago
Decq, Louise, Frederic Lynen, Michael Schilling, Wim Fremout, Vincent Cattersel, Delphine Steyaert, Charles Indekeu, Emile Van Binnebeke, and Steven Saverwyns. 2016. “The Analysis of European Lacquer : Optimization of Thermochemolysis Temperature of Natural Resins.” Applied Physics A-materials Science & Processing 122 (12).
APA
Decq, L., Lynen, F., Schilling, M., Fremout, W., Cattersel, V., Steyaert, D., Indekeu, C., et al. (2016). The analysis of European lacquer : optimization of thermochemolysis temperature of natural resins. APPLIED PHYSICS A-MATERIALS SCIENCE & PROCESSING, 122(12).
Vancouver
1.
Decq L, Lynen F, Schilling M, Fremout W, Cattersel V, Steyaert D, et al. The analysis of European lacquer : optimization of thermochemolysis temperature of natural resins. APPLIED PHYSICS A-MATERIALS SCIENCE & PROCESSING. 2016;122(12).
MLA
Decq, Louise, Frederic Lynen, Michael Schilling, et al. “The Analysis of European Lacquer : Optimization of Thermochemolysis Temperature of Natural Resins.” APPLIED PHYSICS A-MATERIALS SCIENCE & PROCESSING 122.12 (2016): n. pag. Print.