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Scalable heating-up synthesis of monodisperse Cu2ZnSnS4 nanocrystals

(2016) CHEMISTRY OF MATERIALS. 28(3). p.720-726
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Abstract
Monodisperse Cu2ZnSnS4 (CZTS) nanocrystals (NCs), with quasi spherical shape, were prepared by a facile, high-yield, scalable, and high-concentration heat-up procedure. The key parameters to minimize the NC size distribution were efficient mixing and heat transfer in the reaction mixture through intensive argon bubbling and improved control of the heating ramp stability. Optimized synthetic conditions allowed the production of several grams of highly monodisperse CZTS NCs per batch, with up to 5 wt % concentration in a crude solution and a yield above 90%.
Keywords
THERMOELECTRIC PROPERTIES, SURFACE-CHEMISTRY, COLLOIDAL NANOCRYSTALS, KESTERITE CU2ZNSNS4, OXIDE NANOCRYSTALS, SOLAR-CELLS, NANOPARTICLES, WURTZITE, FACILE, DIFFUSION

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Citation

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MLA
Shavel, Alexey, et al. “Scalable Heating-up Synthesis of Monodisperse Cu2ZnSnS4 Nanocrystals.” CHEMISTRY OF MATERIALS, vol. 28, no. 3, 2016, pp. 720–26.
APA
Shavel, A., Ibanez, M., Luo, Z., De Roo, J., Carrete, A., Dimitrievska, M., … Cabot, A. (2016). Scalable heating-up synthesis of monodisperse Cu2ZnSnS4 nanocrystals. CHEMISTRY OF MATERIALS, 28(3), 720–726.
Chicago author-date
Shavel, Alexey, Maria Ibanez, Zhishan Luo, Jonathan De Roo, Alex Carrete, Mirjana Dimitrievska, Aziz Genc, et al. 2016. “Scalable Heating-up Synthesis of Monodisperse Cu2ZnSnS4 Nanocrystals.” CHEMISTRY OF MATERIALS 28 (3): 720–26.
Chicago author-date (all authors)
Shavel, Alexey, Maria Ibanez, Zhishan Luo, Jonathan De Roo, Alex Carrete, Mirjana Dimitrievska, Aziz Genc, Michaela Meyns, Alejandro Perez-Rodriguez, Maksym V Kovalenko, Jordi Arbiol, and Andreu Cabot. 2016. “Scalable Heating-up Synthesis of Monodisperse Cu2ZnSnS4 Nanocrystals.” CHEMISTRY OF MATERIALS 28 (3): 720–726.
Vancouver
1.
Shavel A, Ibanez M, Luo Z, De Roo J, Carrete A, Dimitrievska M, et al. Scalable heating-up synthesis of monodisperse Cu2ZnSnS4 nanocrystals. CHEMISTRY OF MATERIALS. 2016;28(3):720–6.
IEEE
[1]
A. Shavel et al., “Scalable heating-up synthesis of monodisperse Cu2ZnSnS4 nanocrystals,” CHEMISTRY OF MATERIALS, vol. 28, no. 3, pp. 720–726, 2016.
@article{7208281,
  abstract     = {Monodisperse Cu2ZnSnS4 (CZTS) nanocrystals (NCs), with quasi spherical shape, were prepared by a facile, high-yield, scalable, and high-concentration heat-up procedure. The key parameters to minimize the NC size distribution were efficient mixing and heat transfer in the reaction mixture through intensive argon bubbling and improved control of the heating ramp stability. Optimized synthetic conditions allowed the production of several grams of highly monodisperse CZTS NCs per batch, with up to 5 wt % concentration in a crude solution and a yield above 90%.},
  author       = {Shavel, Alexey and Ibanez, Maria and Luo, Zhishan and De Roo, Jonathan and Carrete, Alex and Dimitrievska, Mirjana and Genc, Aziz and Meyns, Michaela and Perez-Rodriguez, Alejandro and Kovalenko, Maksym V and Arbiol, Jordi and Cabot, Andreu},
  issn         = {0897-4756},
  journal      = {CHEMISTRY OF MATERIALS},
  keywords     = {THERMOELECTRIC PROPERTIES,SURFACE-CHEMISTRY,COLLOIDAL NANOCRYSTALS,KESTERITE CU2ZNSNS4,OXIDE NANOCRYSTALS,SOLAR-CELLS,NANOPARTICLES,WURTZITE,FACILE,DIFFUSION},
  language     = {eng},
  number       = {3},
  pages        = {720--726},
  title        = {Scalable heating-up synthesis of monodisperse Cu2ZnSnS4 nanocrystals},
  url          = {http://dx.doi.org/10.1021/acs.chemmater.5b03417},
  volume       = {28},
  year         = {2016},
}

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