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Determination of the acaricide fenbutatin oxide in water samples by automated headspace-SPME-GC/MS

Christophe Devos, Luc Moens UGent and Patrick Sandra UGent (2005) JOURNAL OF SEPARATION SCIENCE. 28(7). p.665-668
abstract
The analysis of the acaricide fenbutatin oxide (FBTO) having a molecular weight of 1052.66 g mol(-1) in water samples by capillary GC/MS after in-situ derivatization with sodium tetraethylborate (NaBEt4) and headspace-SPME enrichment is described. Automated SPME is performed at 80° C for 30 min. Detection is carried out in the ion monitoring mode with deuterated triphenyltin (TPhTd15) as internal standard. Good linearity (R-2 = 0.9993) was obtained in the dynamic range 20 to 1000 ng L-1 with a limit of detection of 16 ng L-1 (LOD at 3 S/N) and a limit of quantitation of 50 ng L-1 (LOQ at 10 S/N). Intra-day RSD% for n = 6 was 8.9 at the LOO level.
Please use this url to cite or link to this publication:
author
organization
year
type
journalArticle (original)
publication status
published
subject
keyword
automated headspace-SPME, capillary GC/MS, derivatization, fenbutatin oxide, water samples, SOLID-PHASE MICROEXTRACTION, GAS-CHROMATOGRAPHY, ORGANOTIN COMPOUNDS, MASS-SPECTROMETRY, ENVIRONMENTAL-SAMPLES, EMISSION-SPECTROMETRY, SPECIATION ANALYSIS, GC, FENTIN
journal title
JOURNAL OF SEPARATION SCIENCE
J. Sep. Sci.
volume
28
issue
7
pages
665 - 668
Web of Science type
Article
Web of Science id
000229160400010
JCR category
CHEMISTRY, ANALYTICAL
JCR impact factor
1.829 (2005)
JCR rank
23/69 (2005)
JCR quartile
2 (2005)
ISSN
1615-9306
DOI
10.1002/jssc.200400105
language
English
UGent publication?
yes
classification
A1
copyright statement
I have transferred the copyright for this publication to the publisher
id
340509
handle
http://hdl.handle.net/1854/LU-340509
date created
2006-06-16 14:02:00
date last changed
2012-11-12 13:21:30
@article{340509,
  abstract     = {The analysis of the acaricide fenbutatin oxide (FBTO) having a molecular weight of 1052.66 g mol(-1) in water samples by capillary GC/MS after in-situ derivatization with sodium tetraethylborate (NaBEt4) and headspace-SPME enrichment is described. Automated SPME is performed at 80\° C for 30 min. Detection is carried out in the ion monitoring mode with deuterated triphenyltin (TPhTd15) as internal standard. Good linearity (R-2 = 0.9993) was obtained in the dynamic range 20 to 1000 ng L-1 with a limit of detection of 16 ng L-1 (LOD at 3 S/N) and a limit of quantitation of 50 ng L-1 (LOQ at 10 S/N). Intra-day RSD\% for n = 6 was 8.9 at the LOO level.},
  author       = {Devos, Christophe and Moens, Luc and Sandra, Patrick},
  issn         = {1615-9306},
  journal      = {JOURNAL OF SEPARATION SCIENCE},
  keyword      = {automated headspace-SPME,capillary GC/MS,derivatization,fenbutatin oxide,water samples,SOLID-PHASE MICROEXTRACTION,GAS-CHROMATOGRAPHY,ORGANOTIN COMPOUNDS,MASS-SPECTROMETRY,ENVIRONMENTAL-SAMPLES,EMISSION-SPECTROMETRY,SPECIATION ANALYSIS,GC,FENTIN},
  language     = {eng},
  number       = {7},
  pages        = {665--668},
  title        = {Determination of the acaricide fenbutatin oxide in water samples by automated headspace-SPME-GC/MS},
  url          = {http://dx.doi.org/10.1002/jssc.200400105},
  volume       = {28},
  year         = {2005},
}

Chicago
Devos, Christophe, Luc Moens, and Patrick Sandra. 2005. “Determination of the Acaricide Fenbutatin Oxide in Water Samples by Automated headspace-SPME-GC/MS.” Journal of Separation Science 28 (7): 665–668.
APA
Devos, Christophe, Moens, L., & Sandra, P. (2005). Determination of the acaricide fenbutatin oxide in water samples by automated headspace-SPME-GC/MS. JOURNAL OF SEPARATION SCIENCE, 28(7), 665–668.
Vancouver
1.
Devos C, Moens L, Sandra P. Determination of the acaricide fenbutatin oxide in water samples by automated headspace-SPME-GC/MS. JOURNAL OF SEPARATION SCIENCE. 2005;28(7):665–8.
MLA
Devos, Christophe, Luc Moens, and Patrick Sandra. “Determination of the Acaricide Fenbutatin Oxide in Water Samples by Automated headspace-SPME-GC/MS.” JOURNAL OF SEPARATION SCIENCE 28.7 (2005): 665–668. Print.