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LC-MS N-alkylamide profiling of an ethanolic Anacyclus pyrethrum root extract

Jente Boonen UGent, Vikas Sharma, Vinod Dixit, Christian Burvenich UGent and Bart De Spiegeleer UGent (2012) PLANTA MEDICA. 78(16). p.1787-1795
abstract
An N-alkylamide profiling from an ethanolic Anacyclus pyrethrum DC. (Asteraceae) root extract was performed using a gradient reversed phase high performance liquid chromatography/UV/electrospray-ionization ion-trap mass spectrometry (HPLC/UV/ESI-MS) method on an embedded polar column. MS1 and MS2 32 fragmentation data were used for identification purposes, while UV was used for quantification. Thirteen N-alkylamides (five N-isobutylamides, three N-methyl isobutylamides, four tyramides and one 2-phenylethylamide) were detected. Six of them, identified as undeca-2E,4E-diene-8,10-diynoic acid isobutylamide, undeca-2E,4E-diene-8,10-diynoic acid N-methyl isobutylamide, tetradeca-2E,4E-diene-8,10-diynoic acid tyramide, deca-2E,4E-dienoic acid N-methyl isobutylamide, tetradeca-2E,4E,XE/Z-trienoic acid tyramide and tetradeca-2E,4E,XE/Z,YE/Z-tetraenoic isobutylamide, are novel compounds which have never been reported before in Anacyclus pyrethrum.
Please use this url to cite or link to this publication:
author
organization
year
type
journalArticle (original)
publication status
published
subject
keyword
pellitorine, N-alkylamides, LC-MS plant profiling, Anacyclus pyrethrum (Asteraceae), anacycline
journal title
PLANTA MEDICA
Planta Med.
volume
78
issue
16
pages
1787 - 1795
Web of Science type
Article
Web of Science id
000310779900013
JCR category
PLANT SCIENCES
JCR impact factor
2.348 (2012)
JCR rank
55/193 (2012)
JCR quartile
2 (2012)
ISSN
0032-0943
DOI
10.1055/s-0032-1315371
language
English
UGent publication?
yes
classification
A1
copyright statement
I have transferred the copyright for this publication to the publisher
id
2133823
handle
http://hdl.handle.net/1854/LU-2133823
date created
2012-06-06 09:57:24
date last changed
2013-07-05 13:55:02
@article{2133823,
  abstract     = {An N-alkylamide profiling from an ethanolic Anacyclus pyrethrum DC. (Asteraceae) root extract was performed using a gradient reversed phase high performance liquid chromatography/UV/electrospray-ionization ion-trap mass spectrometry (HPLC/UV/ESI-MS) method on an embedded polar column. MS1 and MS2 32 fragmentation data were used for  identification purposes, while UV was used for quantification. Thirteen N-alkylamides (five N-isobutylamides, three N-methyl isobutylamides, four tyramides and one 2-phenylethylamide) were detected. Six of them, identified as undeca-2E,4E-diene-8,10-diynoic acid isobutylamide, undeca-2E,4E-diene-8,10-diynoic acid N-methyl isobutylamide, tetradeca-2E,4E-diene-8,10-diynoic acid tyramide, deca-2E,4E-dienoic acid N-methyl isobutylamide, tetradeca-2E,4E,XE/Z-trienoic acid tyramide and tetradeca-2E,4E,XE/Z,YE/Z-tetraenoic isobutylamide, are novel compounds which have never been reported before in Anacyclus pyrethrum.},
  author       = {Boonen, Jente and Sharma, Vikas and Dixit, Vinod and Burvenich, Christian and De Spiegeleer, Bart},
  issn         = {0032-0943},
  journal      = {PLANTA MEDICA},
  keyword      = {pellitorine,N-alkylamides,LC-MS plant profiling,Anacyclus pyrethrum (Asteraceae),anacycline},
  language     = {eng},
  number       = {16},
  pages        = {1787--1795},
  title        = {LC-MS N-alkylamide profiling of an ethanolic Anacyclus pyrethrum root extract},
  url          = {http://dx.doi.org/10.1055/s-0032-1315371},
  volume       = {78},
  year         = {2012},
}

Chicago
Boonen, Jente, Vikas Sharma, Vinod Dixit, Christian Burvenich, and Bart De Spiegeleer. 2012. “LC-MS N-alkylamide Profiling of an Ethanolic Anacyclus Pyrethrum Root Extract.” Planta Medica 78 (16): 1787–1795.
APA
Boonen, J., Sharma, V., Dixit, V., Burvenich, C., & De Spiegeleer, B. (2012). LC-MS N-alkylamide profiling of an ethanolic Anacyclus pyrethrum root extract. PLANTA MEDICA, 78(16), 1787–1795.
Vancouver
1.
Boonen J, Sharma V, Dixit V, Burvenich C, De Spiegeleer B. LC-MS N-alkylamide profiling of an ethanolic Anacyclus pyrethrum root extract. PLANTA MEDICA. 2012;78(16):1787–95.
MLA
Boonen, Jente, Vikas Sharma, Vinod Dixit, et al. “LC-MS N-alkylamide Profiling of an Ethanolic Anacyclus Pyrethrum Root Extract.” PLANTA MEDICA 78.16 (2012): 1787–1795. Print.