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Ordered mesoporous silica materials in liquid chromatography: synthesis and application

Matthias Ide UGent (2012)
abstract
This research work describes the synthesis and application of ordered mesoporous silica materials in liquid chromatography. For this purpose spherical particles and thick layers were developed. In a first part the synthesis and the particle properties were investigated. Spray drying was used as a fast technique to produce sufficient quantities of spherical ordered mesoporous particles. After the proces was optimized adequate amounts of both an organosilica and a pure silica material were packed and chromatographically evaluated. The ordered porosity as it seems has a profound influence on the retention of analytes as it more than triples. The second and final part describes the synthesis of a thick layer on the inner lining of a fused silica capillary. This open tubular column was evaluated in capillary electro chromatography where various mixtures were succesfully base separated.
Please use this url to cite or link to this publication:
author
promoter
UGent and UGent
organization
year
type
dissertation (monograph)
subject
pages
XX, 206 pages
publisher
Ghent University. Faculty of Sciences
place of publication
Ghent, Belgium
defense location
Gent : Het Pand
defense date
2012-03-16 15:00
language
English
UGent publication?
yes
classification
D1
copyright statement
I have retained and own the full copyright for this publication
id
2072660
handle
http://hdl.handle.net/1854/LU-2072660
date created
2012-03-22 14:23:46
date last changed
2014-03-01 00:30:47
@phdthesis{2072660,
  abstract     = {This research work describes the synthesis and application of ordered mesoporous silica materials in liquid chromatography. For this purpose spherical particles and thick layers were developed.
In a first part the synthesis and the particle properties were investigated. Spray drying was used as a fast technique to produce sufficient quantities of spherical ordered mesoporous particles. After the proces was optimized adequate amounts of both an organosilica and a pure silica material were packed and chromatographically evaluated. The ordered porosity as it seems has a profound influence on the retention of analytes as it more than triples.
The second and final part describes the synthesis of a thick layer on the inner lining of a fused silica capillary. This open tubular column was evaluated in capillary electro chromatography where various mixtures were succesfully base separated.},
  author       = {Ide, Matthias},
  language     = {eng},
  pages        = {XX, 206},
  publisher    = {Ghent University. Faculty of Sciences},
  school       = {Ghent University},
  title        = {Ordered mesoporous silica materials in liquid chromatography: synthesis and application},
  year         = {2012},
}

Chicago
Ide, Matthias. 2012. “Ordered Mesoporous Silica Materials in Liquid Chromatography: Synthesis and Application”. Ghent, Belgium: Ghent University. Faculty of Sciences.
APA
Ide, Matthias. (2012). Ordered mesoporous silica materials in liquid chromatography: synthesis and application. Ghent University. Faculty of Sciences, Ghent, Belgium.
Vancouver
1.
Ide M. Ordered mesoporous silica materials in liquid chromatography: synthesis and application. [Ghent, Belgium]: Ghent University. Faculty of Sciences; 2012.
MLA
Ide, Matthias. “Ordered Mesoporous Silica Materials in Liquid Chromatography: Synthesis and Application.” 2012 : n. pag. Print.