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Ordered mesoporous silica materials in liquid chromatography: synthesis and application

Matthias Ide (UGent)
(2012)
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(UGent) and (UGent)
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Abstract
This research work describes the synthesis and application of ordered mesoporous silica materials in liquid chromatography. For this purpose spherical particles and thick layers were developed. In a first part the synthesis and the particle properties were investigated. Spray drying was used as a fast technique to produce sufficient quantities of spherical ordered mesoporous particles. After the proces was optimized adequate amounts of both an organosilica and a pure silica material were packed and chromatographically evaluated. The ordered porosity as it seems has a profound influence on the retention of analytes as it more than triples. The second and final part describes the synthesis of a thick layer on the inner lining of a fused silica capillary. This open tubular column was evaluated in capillary electro chromatography where various mixtures were succesfully base separated.

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Citation

Please use this url to cite or link to this publication:

Chicago
Ide, Matthias. 2012. “Ordered Mesoporous Silica Materials in Liquid Chromatography: Synthesis and Application”. Ghent, Belgium: Ghent University. Faculty of Sciences.
APA
Ide, Matthias. (2012). Ordered mesoporous silica materials in liquid chromatography: synthesis and application. Ghent University. Faculty of Sciences, Ghent, Belgium.
Vancouver
1.
Ide M. Ordered mesoporous silica materials in liquid chromatography: synthesis and application. [Ghent, Belgium]: Ghent University. Faculty of Sciences; 2012.
MLA
Ide, Matthias. “Ordered Mesoporous Silica Materials in Liquid Chromatography: Synthesis and Application.” 2012 : n. pag. Print.
@phdthesis{2072660,
  abstract     = {This research work describes the synthesis and application of ordered mesoporous silica materials in liquid chromatography. For this purpose spherical particles and thick layers were developed.
In a first part the synthesis and the particle properties were investigated. Spray drying was used as a fast technique to produce sufficient quantities of spherical ordered mesoporous particles. After the proces was optimized adequate amounts of both an organosilica and a pure silica material were packed and chromatographically evaluated. The ordered porosity as it seems has a profound influence on the retention of analytes as it more than triples.
The second and final part describes the synthesis of a thick layer on the inner lining of a fused silica capillary. This open tubular column was evaluated in capillary electro chromatography where various mixtures were succesfully base separated.},
  author       = {Ide, Matthias},
  language     = {eng},
  pages        = {XX, 206},
  publisher    = {Ghent University. Faculty of Sciences},
  school       = {Ghent University},
  title        = {Ordered mesoporous silica materials in liquid chromatography: synthesis and application},
  year         = {2012},
}