- Author
- Matthias Ide (UGent)
- Promoter
- Pascal Van Der Voort (UGent) and Patrick Sandra (UGent)
- Organization
- Abstract
- This research work describes the synthesis and application of ordered mesoporous silica materials in liquid chromatography. For this purpose spherical particles and thick layers were developed. In a first part the synthesis and the particle properties were investigated. Spray drying was used as a fast technique to produce sufficient quantities of spherical ordered mesoporous particles. After the proces was optimized adequate amounts of both an organosilica and a pure silica material were packed and chromatographically evaluated. The ordered porosity as it seems has a profound influence on the retention of analytes as it more than triples. The second and final part describes the synthesis of a thick layer on the inner lining of a fused silica capillary. This open tubular column was evaluated in capillary electro chromatography where various mixtures were succesfully base separated.
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Citation
Please use this url to cite or link to this publication: http://hdl.handle.net/1854/LU-2072660
- MLA
- Ide, Matthias. Ordered Mesoporous Silica Materials in Liquid Chromatography : Synthesis and Application. Ghent University. Faculty of Sciences, 2012.
- APA
- Ide, M. (2012). Ordered mesoporous silica materials in liquid chromatography : synthesis and application. Ghent University. Faculty of Sciences, Ghent, Belgium.
- Chicago author-date
- Ide, Matthias. 2012. “Ordered Mesoporous Silica Materials in Liquid Chromatography : Synthesis and Application.” Ghent, Belgium: Ghent University. Faculty of Sciences.
- Chicago author-date (all authors)
- Ide, Matthias. 2012. “Ordered Mesoporous Silica Materials in Liquid Chromatography : Synthesis and Application.” Ghent, Belgium: Ghent University. Faculty of Sciences.
- Vancouver
- 1.Ide M. Ordered mesoporous silica materials in liquid chromatography : synthesis and application. [Ghent, Belgium]: Ghent University. Faculty of Sciences; 2012.
- IEEE
- [1]M. Ide, “Ordered mesoporous silica materials in liquid chromatography : synthesis and application,” Ghent University. Faculty of Sciences, Ghent, Belgium, 2012.
@phdthesis{2072660, abstract = {{This research work describes the synthesis and application of ordered mesoporous silica materials in liquid chromatography. For this purpose spherical particles and thick layers were developed. In a first part the synthesis and the particle properties were investigated. Spray drying was used as a fast technique to produce sufficient quantities of spherical ordered mesoporous particles. After the proces was optimized adequate amounts of both an organosilica and a pure silica material were packed and chromatographically evaluated. The ordered porosity as it seems has a profound influence on the retention of analytes as it more than triples. The second and final part describes the synthesis of a thick layer on the inner lining of a fused silica capillary. This open tubular column was evaluated in capillary electro chromatography where various mixtures were succesfully base separated.}}, author = {{Ide, Matthias}}, language = {{eng}}, pages = {{XX, 206}}, publisher = {{Ghent University. Faculty of Sciences}}, school = {{Ghent University}}, title = {{Ordered mesoporous silica materials in liquid chromatography : synthesis and application}}, year = {{2012}}, }