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Accelerated solid-phase dynamic extraction for the analysis of biogenic volatile organic compounds in air

Olga Pokorska UGent, Jo Dewulf UGent and Herman Van Langenhove UGent (2011) INTERNATIONAL JOURNAL OF ENVIRONMENTAL ANALYTICAL CHEMISTRY. 91(12). p.1206-1217
abstract
In this study, accelerated solid phase dynamic extraction (ASPDE) technique was used to identify biogenic volatile organic compounds (BVOCs) emitted from Norway spruce (Picea abies). Compounds that were determined in tree samples are: tricycylene, alpha-pinene, camphene, beta-pinene, myrcene, 3-carene, p-cymene, limonene, cineole, alpha-phellandrene, alpha-terpinene, gamma-terpinene and terpinolene. ASPDE showed a potential for the analysis of environmental samples as well as for field applications. This technique was further studied by using a gaseous mixture of BVOCs (sabinene, alpha-pinene, beta-pinene, limonene, linalool, and (Z)-hexenyl acetate) and exhibited a good repeatability during all the experiments in the range of 2.5% (alpha-pinene) and 14.6% (linalool). However, during the analysis of samples it was observed that desorption at high temperature (230 degrees C) can lead to the formation of artifacts, which were not observed at the desorption temperature of 100 degrees C. Further experimental investigations revealed that monoterpenes appeared as unanticipated compounds during desorption of ASPDE samples; these compounds were degradation products of linalool.
Please use this url to cite or link to this publication:
author
organization
year
type
journalArticle (original)
publication status
published
subject
keyword
preconcentration techniques, accelerated solid phase dynamic extraction, biogenic volatile organic compounds, environmental monitoring, GAS CHROMATOGRAPHY/MASS SPECTROMETRY, HAIR SAMPLES, MONOTERPENE EMISSIONS, ISOPRENE EMISSIONS, MICROEXTRACTION, SCOTS PINE, TOLUENE, WATER, SESQUITERPENE, ETHYLBENZENE
journal title
INTERNATIONAL JOURNAL OF ENVIRONMENTAL ANALYTICAL CHEMISTRY
Int. J. Environ. Anal. Chem.
volume
91
issue
12
pages
1206 - 1217
Web of Science type
Article
Web of Science id
000297261400007
JCR category
ENVIRONMENTAL SCIENCES
JCR impact factor
1.162 (2011)
JCR rank
133/203 (2011)
JCR quartile
3 (2011)
ISSN
0306-7319
DOI
10.1080/03067311003778656
language
English
UGent publication?
yes
classification
A1
copyright statement
I have transferred the copyright for this publication to the publisher
id
2020891
handle
http://hdl.handle.net/1854/LU-2020891
date created
2012-02-06 16:22:42
date last changed
2012-02-06 16:49:48
@article{2020891,
  abstract     = {In this study, accelerated solid phase dynamic extraction (ASPDE) technique was used to identify biogenic volatile organic compounds (BVOCs) emitted from Norway spruce (Picea abies). Compounds that were determined in tree samples are: tricycylene, alpha-pinene, camphene, beta-pinene, myrcene, 3-carene, p-cymene, limonene, cineole, alpha-phellandrene, alpha-terpinene, gamma-terpinene and terpinolene. ASPDE showed a potential for the analysis of environmental samples as well as for field applications. This technique was further studied by using a gaseous mixture of BVOCs (sabinene, alpha-pinene, beta-pinene, limonene, linalool, and (Z)-hexenyl acetate) and exhibited a good repeatability during all the experiments in the range of 2.5\% (alpha-pinene) and 14.6\% (linalool). However, during the analysis of samples it was observed that desorption at high temperature (230 degrees C) can lead to the formation of artifacts, which were not observed at the desorption temperature of 100 degrees C. Further experimental investigations revealed that monoterpenes appeared as unanticipated compounds during desorption of ASPDE samples; these compounds were degradation products of linalool.},
  author       = {Pokorska, Olga and Dewulf, Jo and Van Langenhove, Herman},
  issn         = {0306-7319},
  journal      = {INTERNATIONAL JOURNAL OF ENVIRONMENTAL ANALYTICAL CHEMISTRY},
  keyword      = {preconcentration techniques,accelerated solid phase dynamic extraction,biogenic volatile organic compounds,environmental monitoring,GAS CHROMATOGRAPHY/MASS SPECTROMETRY,HAIR SAMPLES,MONOTERPENE EMISSIONS,ISOPRENE EMISSIONS,MICROEXTRACTION,SCOTS PINE,TOLUENE,WATER,SESQUITERPENE,ETHYLBENZENE},
  language     = {eng},
  number       = {12},
  pages        = {1206--1217},
  title        = {Accelerated solid-phase dynamic extraction for the analysis of biogenic volatile organic compounds in air},
  url          = {http://dx.doi.org/10.1080/03067311003778656},
  volume       = {91},
  year         = {2011},
}

Chicago
Pokorska, Olga, Jo Dewulf, and Herman Van Langenhove. 2011. “Accelerated Solid-phase Dynamic Extraction for the Analysis of Biogenic Volatile Organic Compounds in Air.” International Journal of Environmental Analytical Chemistry 91 (12): 1206–1217.
APA
Pokorska, O., Dewulf, J., & Van Langenhove, H. (2011). Accelerated solid-phase dynamic extraction for the analysis of biogenic volatile organic compounds in air. INTERNATIONAL JOURNAL OF ENVIRONMENTAL ANALYTICAL CHEMISTRY, 91(12), 1206–1217.
Vancouver
1.
Pokorska O, Dewulf J, Van Langenhove H. Accelerated solid-phase dynamic extraction for the analysis of biogenic volatile organic compounds in air. INTERNATIONAL JOURNAL OF ENVIRONMENTAL ANALYTICAL CHEMISTRY. 2011;91(12):1206–17.
MLA
Pokorska, Olga, Jo Dewulf, and Herman Van Langenhove. “Accelerated Solid-phase Dynamic Extraction for the Analysis of Biogenic Volatile Organic Compounds in Air.” INTERNATIONAL JOURNAL OF ENVIRONMENTAL ANALYTICAL CHEMISTRY 91.12 (2011): 1206–1217. Print.