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A statistical Plackett-Burman design of the thermal process in the synthesis of the Bi-2223 HTSC

Author
Organization
Abstract
In this study, the most significant parameters in the thermal process for the preparation of high-quality Bi-2223 HTSCs are determined using a statistical Plackett-Burman screening design. This enabled us to obtain a quick and objective evaluation, where the significant parameters could be unambiguously defined, accounting for interactions with other parameters. Using the optimal conditions of the thermal process and starting from a spray dried nitrate solution with nominal composition Bi:Pb:Sr:Ca:Cu = 1.5:0.5:2:3:4, a more than 96% pure Bi-2223 phase (relative to the Bi-2212 phase) could be synthesized in a minimal thermal process of 5 h calcination at 650 degrees C and 60 h sintering at 855 degrees C.
Keywords
HIGH-TC PHASE, CU-O SYSTEM, BI

Citation

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MLA
Van Driessche, Isabel, F Persyn, Lucien Fiermans, et al. “A Statistical Plackett-Burman Design of the Thermal Process in the Synthesis of the Bi-2223 HTSC.” SUPERCONDUCTOR SCIENCE & TECHNOLOGY 9.10 (1996): 843–848. Print.
APA
Van Driessche, I., Persyn, F., Fiermans, L., & Hoste, S. (1996). A statistical Plackett-Burman design of the thermal process in the synthesis of the Bi-2223 HTSC. SUPERCONDUCTOR SCIENCE & TECHNOLOGY, 9(10), 843–848.
Chicago author-date
Van Driessche, Isabel, F Persyn, Lucien Fiermans, and Serge Hoste. 1996. “A Statistical Plackett-Burman Design of the Thermal Process in the Synthesis of the Bi-2223 HTSC.” Superconductor Science & Technology 9 (10): 843–848.
Chicago author-date (all authors)
Van Driessche, Isabel, F Persyn, Lucien Fiermans, and Serge Hoste. 1996. “A Statistical Plackett-Burman Design of the Thermal Process in the Synthesis of the Bi-2223 HTSC.” Superconductor Science & Technology 9 (10): 843–848.
Vancouver
1.
Van Driessche I, Persyn F, Fiermans L, Hoste S. A statistical Plackett-Burman design of the thermal process in the synthesis of the Bi-2223 HTSC. SUPERCONDUCTOR SCIENCE & TECHNOLOGY. 1996;9(10):843–8.
IEEE
[1]
I. Van Driessche, F. Persyn, L. Fiermans, and S. Hoste, “A statistical Plackett-Burman design of the thermal process in the synthesis of the Bi-2223 HTSC,” SUPERCONDUCTOR SCIENCE & TECHNOLOGY, vol. 9, no. 10, pp. 843–848, 1996.
@article{190379,
  abstract     = {In this study, the most significant parameters in the thermal process for the preparation of high-quality Bi-2223 HTSCs are determined using a statistical Plackett-Burman screening design. This enabled us to obtain a quick and objective evaluation, where the significant parameters could be unambiguously defined, accounting for interactions with other parameters. Using the optimal conditions of the thermal process and starting from a spray dried nitrate solution with nominal composition Bi:Pb:Sr:Ca:Cu = 1.5:0.5:2:3:4, a more than 96% pure Bi-2223 phase (relative to the Bi-2212 phase) could be synthesized in a minimal thermal process of 5 h calcination at 650 degrees C and 60 h sintering at 855 degrees C.},
  author       = {Van Driessche, Isabel and Persyn, F and Fiermans, Lucien and Hoste, Serge},
  issn         = {0953-2048},
  journal      = {SUPERCONDUCTOR SCIENCE & TECHNOLOGY},
  keywords     = {HIGH-TC PHASE,CU-O SYSTEM,BI},
  language     = {eng},
  number       = {10},
  pages        = {843--848},
  title        = {A statistical Plackett-Burman design of the thermal process in the synthesis of the Bi-2223 HTSC},
  volume       = {9},
  year         = {1996},
}