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Spectral X-ray computed tomography for the chemical identification of critical minerals

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Abstract
Differentiating minerals using high-resolution X-ray tomography (µCT) relies on distinct differences in the attenuation coefficient µ. The µ value depends on an interplay between the material density ρ and the effective atomic number Zeff of a mineral phase. Difficulties in identifying mineral phases arise when this interplay gives similar µ values and thus limited contrast within µCT images. Untangling these two dependencies is essential to improve the three-dimensional chemical identification of critical minerals. Lab-based methods and techniques often incorporate different measures, but only show a limited application potential on multiphase geological samples. Using high-Z spectral laboratory-based µCT we studied the potential of directly identifying chemical elements within the practical margins of high-Z spectral detectors. This paper compares the results from three mineral deposits using two spectral µCT setups. Chemical elements with a Z higher than molybdenum and a concentration of at least some weight percentage were correctly identified using K-edge imaging. The suitability of the different high-Z spectral detectors depends largely on the availability of prior knowledge of the sample composition. Quantifying elemental concentrations is element- and sample specific and currently does not allow for optimal automated mineralogy solutions. Improving the three-dimensional identification of minerals can be achieved with dedicated analyses of the energy-dependent µ curve and therefore will remain the focus of future work.
Keywords
Spectral computed tomography, CdTe detector, K-edge imaging, 3D chemistry, Mineral identification, Critical minerals, Economic geology

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MLA
Buyse, Florian, et al. “Spectral X-Ray Computed Tomography for the Chemical Identification of Critical Minerals.” TOMOGRAPHY OF MATERIALS AND STRUCTURES, vol. 8, 2025, doi:10.1016/j.tmater.2025.100059.
APA
Buyse, F., Boone, M., Van Assche, F., Faucher, S., Moonen, P., Dewaele, S., & Cnudde, V. (2025). Spectral X-ray computed tomography for the chemical identification of critical minerals. TOMOGRAPHY OF MATERIALS AND STRUCTURES, 8. https://doi.org/10.1016/j.tmater.2025.100059
Chicago author-date
Buyse, Florian, Matthieu Boone, Frederic Van Assche, Stéphane Faucher, Peter Moonen, Stijn Dewaele, and Veerle Cnudde. 2025. “Spectral X-Ray Computed Tomography for the Chemical Identification of Critical Minerals.” TOMOGRAPHY OF MATERIALS AND STRUCTURES 8. https://doi.org/10.1016/j.tmater.2025.100059.
Chicago author-date (all authors)
Buyse, Florian, Matthieu Boone, Frederic Van Assche, Stéphane Faucher, Peter Moonen, Stijn Dewaele, and Veerle Cnudde. 2025. “Spectral X-Ray Computed Tomography for the Chemical Identification of Critical Minerals.” TOMOGRAPHY OF MATERIALS AND STRUCTURES 8. doi:10.1016/j.tmater.2025.100059.
Vancouver
1.
Buyse F, Boone M, Van Assche F, Faucher S, Moonen P, Dewaele S, et al. Spectral X-ray computed tomography for the chemical identification of critical minerals. TOMOGRAPHY OF MATERIALS AND STRUCTURES. 2025;8.
IEEE
[1]
F. Buyse et al., “Spectral X-ray computed tomography for the chemical identification of critical minerals,” TOMOGRAPHY OF MATERIALS AND STRUCTURES, vol. 8, 2025.
@article{01JNZF9G8NCR9RVJC6WDYX3498,
  abstract     = {{Differentiating minerals using high-resolution X-ray tomography (µCT) relies on distinct differences in the attenuation coefficient µ. The µ value depends on an interplay between the material density ρ and the effective atomic number Zeff of a mineral phase. Difficulties in identifying mineral phases arise when this interplay gives similar µ values and thus limited contrast within µCT images. Untangling these two dependencies is essential to improve the three-dimensional chemical identification of critical minerals. Lab-based methods and techniques often incorporate different measures, but only show a limited application potential on multiphase geological samples. Using high-Z spectral laboratory-based µCT we studied the potential of directly identifying chemical elements within the practical margins of high-Z spectral detectors. This paper compares the results from three mineral deposits using two spectral µCT setups. Chemical elements with a Z higher than molybdenum and a concentration of at least some weight percentage were correctly identified using K-edge imaging. The suitability of the different high-Z spectral detectors depends largely on the availability of prior knowledge of the sample composition. Quantifying elemental concentrations is element- and sample specific and currently does not allow for optimal automated mineralogy solutions. Improving the three-dimensional identification of minerals can be achieved with dedicated analyses of the energy-dependent µ curve and therefore will remain the focus of future work.}},
  articleno    = {{100059}},
  author       = {{Buyse, Florian and Boone, Matthieu and Van Assche, Frederic and Faucher, Stéphane and Moonen, Peter and Dewaele, Stijn and Cnudde, Veerle}},
  issn         = {{2949-673X}},
  journal      = {{TOMOGRAPHY OF MATERIALS AND STRUCTURES}},
  keywords     = {{Spectral computed tomography,CdTe detector,K-edge imaging,3D chemistry,Mineral identification,Critical minerals,Economic geology}},
  language     = {{eng}},
  pages        = {{13}},
  title        = {{Spectral X-ray computed tomography for the chemical identification of critical minerals}},
  url          = {{http://doi.org/10.1016/j.tmater.2025.100059}},
  volume       = {{8}},
  year         = {{2025}},
}

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