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Impact of synthesis parameters on the crystallinity of macroscopic zeolite Y spheres shaped using resin hard templates

(2024) CRYSTALS. 14(12).
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Abstract
In this study, the effects of several synthesis parameters including aging time, micropore-structure-directing agents, and hydrothermal treatment temperature profile were systematically examined with respect to their impact on the crystallinity of macroscopic zeolite Y spheres formed in the presence of organic anion-exchange resin templates. Spherical resins were utilized as hard templates to shape the zeolite Y particles. Zeolite Y precursors were initially deposited into the pores of the resin template and subsequently crystallized over time through precise control over these synthesis parameters. The resulting zeolite Y spheres were characterized using an array of characterization techniques, including XRD, SEM, TEM, BET, FTIR, and XRF. We identify the optimal conditions for maximizing the crystallinity of the macroscopic zeolite Y particles using resin templates as macroscopic shaping agents. This functional material has the potential to be used as both catalyst and adsorbent in several applications.
Keywords
crystallization, macroscopic zeolite Y spheres, hard templating technique, resin template, zeolite shaping, inorganic crystallization, morphological changes, DIFFUSION

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MLA
Asgar Pour, Zahra, et al. “Impact of Synthesis Parameters on the Crystallinity of Macroscopic Zeolite Y Spheres Shaped Using Resin Hard Templates.” CRYSTALS, vol. 14, no. 12, 2024, doi:10.3390/cryst14121051.
APA
Asgar Pour, Z., Abu Zeitoun, E., Alassmy, Y. A., El Hariri El Nokab, M., Van Steenberge, P., & Sebakhy, K. (2024). Impact of synthesis parameters on the crystallinity of macroscopic zeolite Y spheres shaped using resin hard templates. CRYSTALS, 14(12). https://doi.org/10.3390/cryst14121051
Chicago author-date
Asgar Pour, Zahra, Edrees Abu Zeitoun, Yasser A. Alassmy, Mustapha El Hariri El Nokab, Paul Van Steenberge, and Khaled Sebakhy. 2024. “Impact of Synthesis Parameters on the Crystallinity of Macroscopic Zeolite Y Spheres Shaped Using Resin Hard Templates.” CRYSTALS 14 (12). https://doi.org/10.3390/cryst14121051.
Chicago author-date (all authors)
Asgar Pour, Zahra, Edrees Abu Zeitoun, Yasser A. Alassmy, Mustapha El Hariri El Nokab, Paul Van Steenberge, and Khaled Sebakhy. 2024. “Impact of Synthesis Parameters on the Crystallinity of Macroscopic Zeolite Y Spheres Shaped Using Resin Hard Templates.” CRYSTALS 14 (12). doi:10.3390/cryst14121051.
Vancouver
1.
Asgar Pour Z, Abu Zeitoun E, Alassmy YA, El Hariri El Nokab M, Van Steenberge P, Sebakhy K. Impact of synthesis parameters on the crystallinity of macroscopic zeolite Y spheres shaped using resin hard templates. CRYSTALS. 2024;14(12).
IEEE
[1]
Z. Asgar Pour, E. Abu Zeitoun, Y. A. Alassmy, M. El Hariri El Nokab, P. Van Steenberge, and K. Sebakhy, “Impact of synthesis parameters on the crystallinity of macroscopic zeolite Y spheres shaped using resin hard templates,” CRYSTALS, vol. 14, no. 12, 2024.
@article{01JJKANYHHTCNH10D440JD2Y9H,
  abstract     = {{In this study, the effects of several synthesis parameters including aging time, micropore-structure-directing agents, and hydrothermal treatment temperature profile were systematically examined with respect to their impact on the crystallinity of macroscopic zeolite Y spheres formed in the presence of organic anion-exchange resin templates. Spherical resins were utilized as hard templates to shape the zeolite Y particles. Zeolite Y precursors were initially deposited into the pores of the resin template and subsequently crystallized over time through precise control over these synthesis parameters. The resulting zeolite Y spheres were characterized using an array of characterization techniques, including XRD, SEM, TEM, BET, FTIR, and XRF. We identify the optimal conditions for maximizing the crystallinity of the macroscopic zeolite Y particles using resin templates as macroscopic shaping agents. This functional material has the potential to be used as both catalyst and adsorbent in several applications.}},
  articleno    = {{1051}},
  author       = {{Asgar Pour, Zahra and Abu Zeitoun, Edrees and Alassmy, Yasser A. and El Hariri El Nokab, Mustapha and Van Steenberge, Paul and Sebakhy, Khaled}},
  issn         = {{2073-4352}},
  journal      = {{CRYSTALS}},
  keywords     = {{crystallization,macroscopic zeolite Y spheres,hard templating technique,resin template,zeolite shaping,inorganic crystallization,morphological changes,DIFFUSION}},
  language     = {{eng}},
  number       = {{12}},
  pages        = {{13}},
  title        = {{Impact of synthesis parameters on the crystallinity of macroscopic zeolite Y spheres shaped using resin hard templates}},
  url          = {{http://doi.org/10.3390/cryst14121051}},
  volume       = {{14}},
  year         = {{2024}},
}

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