
Investigating the effects of calcination temperature on porous clay heterostructure characteristics
- Author
- Muhammad Kashif (UGent) , Chaeyeon Kang, Tatwadhika Rangin Siddhartha (UGent) , Clovis Awah Che (UGent) , Yaxin Su and Philippe Heynderickx (UGent)
- Organization
- Abstract
- This study focuses on finding the optimal calcination temperature for synthesizing porous clay heterostructures (PCH). PCH was prepared using montmorillonite at different temperatures (200-800 degrees C) in a closed N2 environment. Samples were characterized via N2-physisorption, scanning electron microscope (SEM), Fourier- transform infrared spectroscopy (FTIR), X-ray diffraction (XRD), and thermogravimetric analysis (TGA) to investigate the influence of calcination temperature. Characterizations show that the PCH composite exhibits an increasing surface profile observed by increasing specific surface area, changes in crystalline phases, porous surface, and varied particle size distribution. The position (degree and wavelength) and intensities of minerals and functional groups in PCH shift with temperature, as observed in both FTIR and XRD. This shows that variables such as heating rate, calcination temperature, and environment affect the structural changes in the clay material. In terms of active phase development, structural behavior, and material strength, the correct calcination temperature proved to be crucial.
- Keywords
- Porous clay heterostructures, Montmorillonite, Calcination, N2-physisorption
Downloads
-
240531-Clean version-4th Man-MK-V1.pdf
- full text (Accepted manuscript)
- |
- open access
- |
- |
- 1.73 MB
-
(...).pdf
- full text (Published version)
- |
- UGent only
- |
- |
- 5.31 MB
Citation
Please use this url to cite or link to this publication: http://hdl.handle.net/1854/LU-01J0ZH8H97CNZQGNEG4RHSR918
- MLA
- Kashif, Muhammad, et al. “Investigating the Effects of Calcination Temperature on Porous Clay Heterostructure Characteristics.” VACUUM, vol. 227, 2024, doi:10.1016/j.vacuum.2024.113415.
- APA
- Kashif, M., Kang, C., Siddhartha, T. R., Che, C. A., Su, Y., & Heynderickx, P. (2024). Investigating the effects of calcination temperature on porous clay heterostructure characteristics. VACUUM, 227. https://doi.org/10.1016/j.vacuum.2024.113415
- Chicago author-date
- Kashif, Muhammad, Chaeyeon Kang, Tatwadhika Rangin Siddhartha, Clovis Awah Che, Yaxin Su, and Philippe Heynderickx. 2024. “Investigating the Effects of Calcination Temperature on Porous Clay Heterostructure Characteristics.” VACUUM 227. https://doi.org/10.1016/j.vacuum.2024.113415.
- Chicago author-date (all authors)
- Kashif, Muhammad, Chaeyeon Kang, Tatwadhika Rangin Siddhartha, Clovis Awah Che, Yaxin Su, and Philippe Heynderickx. 2024. “Investigating the Effects of Calcination Temperature on Porous Clay Heterostructure Characteristics.” VACUUM 227. doi:10.1016/j.vacuum.2024.113415.
- Vancouver
- 1.Kashif M, Kang C, Siddhartha TR, Che CA, Su Y, Heynderickx P. Investigating the effects of calcination temperature on porous clay heterostructure characteristics. VACUUM. 2024;227.
- IEEE
- [1]M. Kashif, C. Kang, T. R. Siddhartha, C. A. Che, Y. Su, and P. Heynderickx, “Investigating the effects of calcination temperature on porous clay heterostructure characteristics,” VACUUM, vol. 227, 2024.
@article{01J0ZH8H97CNZQGNEG4RHSR918, abstract = {{This study focuses on finding the optimal calcination temperature for synthesizing porous clay heterostructures (PCH). PCH was prepared using montmorillonite at different temperatures (200-800 degrees C) in a closed N2 environment. Samples were characterized via N2-physisorption, scanning electron microscope (SEM), Fourier- transform infrared spectroscopy (FTIR), X-ray diffraction (XRD), and thermogravimetric analysis (TGA) to investigate the influence of calcination temperature. Characterizations show that the PCH composite exhibits an increasing surface profile observed by increasing specific surface area, changes in crystalline phases, porous surface, and varied particle size distribution. The position (degree and wavelength) and intensities of minerals and functional groups in PCH shift with temperature, as observed in both FTIR and XRD. This shows that variables such as heating rate, calcination temperature, and environment affect the structural changes in the clay material. In terms of active phase development, structural behavior, and material strength, the correct calcination temperature proved to be crucial.}}, articleno = {{113415}}, author = {{Kashif, Muhammad and Kang, Chaeyeon and Siddhartha, Tatwadhika Rangin and Che, Clovis Awah and Su, Yaxin and Heynderickx, Philippe}}, issn = {{0042-207X}}, journal = {{VACUUM}}, keywords = {{Porous clay heterostructures,Montmorillonite,Calcination,N2-physisorption}}, language = {{eng}}, pages = {{7}}, title = {{Investigating the effects of calcination temperature on porous clay heterostructure characteristics}}, url = {{http://doi.org/10.1016/j.vacuum.2024.113415}}, volume = {{227}}, year = {{2024}}, }
- Altmetric
- View in Altmetric
- Web of Science
- Times cited: