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Implementation of a dual-phase grating interferometer for multi-scale characterization of building materials by tunable dark-field imaging

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Abstract
The multi-scale characterization of building materials is necessary to understand complex mechanical processes, with the goal of developing new more sustainable materials. To that end, imaging methods are often used in materials science to characterize the microscale. However, these methods compromise the volume of interest to achieve a higher resolution. Dark-field (DF) contrast imaging is being investigated to characterize building materials in length scales smaller than the resolution of the imaging system, allowing a direct comparison of features in the nano-scale range and overcoming the scale limitations of the established characterization methods. This work extends the implementation of a dual-phase X-ray grating interferometer (DP-XGI) for DF imaging in a lab-based setup. The interferometer was developed to operate at two different design energies of 22.0 keV and 40.8 keV and was designed to characterize nanoscale-size features in millimeter-sized material samples. The good performance of the interferometer in the low energy range (LER) is demonstrated by the DF retrieval of natural wood samples. In addition, a high energy range (HER) configuration is proposed, resulting in higher mean visibility and good sensitivity over a wider range of correlation lengths in the nanoscale range. Its potential for the characterization of mineral building materials is illustrated by the DF imaging of a Ketton limestone. Additionally, the capability of the DP-XGI to differentiate features in the nanoscale range is proven with the dark-field of Silica nanoparticles at different correlation lengths of calibrated sizes of 106 nm, 261 nm, and 507 nm.
Keywords
Multidisciplinary, RED PINE, RAY, CONTRAST, VISIBILITY, SYSTEMS

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MLA
Organista Castelblanco, Caori, et al. “Implementation of a Dual-Phase Grating Interferometer for Multi-Scale Characterization of Building Materials by Tunable Dark-Field Imaging.” SCIENTIFIC REPORTS, vol. 14, no. 1, 2024, doi:10.1038/s41598-023-50424-6.
APA
Organista Castelblanco, C., Tang, R., Shi, Z., Jefimovs, K., Josell, D., Romano, L., … Boone, M. (2024). Implementation of a dual-phase grating interferometer for multi-scale characterization of building materials by tunable dark-field imaging. SCIENTIFIC REPORTS, 14(1). https://doi.org/10.1038/s41598-023-50424-6
Chicago author-date
Organista Castelblanco, Caori, Ruizhi Tang, Zhitian Shi, Konstantins Jefimovs, Daniel Josell, Lucia Romano, Simon Spindler, et al. 2024. “Implementation of a Dual-Phase Grating Interferometer for Multi-Scale Characterization of Building Materials by Tunable Dark-Field Imaging.” SCIENTIFIC REPORTS 14 (1). https://doi.org/10.1038/s41598-023-50424-6.
Chicago author-date (all authors)
Organista Castelblanco, Caori, Ruizhi Tang, Zhitian Shi, Konstantins Jefimovs, Daniel Josell, Lucia Romano, Simon Spindler, Pierre Kibleur, Benjamin Blykers, Marco Stampanoni, and Matthieu Boone. 2024. “Implementation of a Dual-Phase Grating Interferometer for Multi-Scale Characterization of Building Materials by Tunable Dark-Field Imaging.” SCIENTIFIC REPORTS 14 (1). doi:10.1038/s41598-023-50424-6.
Vancouver
1.
Organista Castelblanco C, Tang R, Shi Z, Jefimovs K, Josell D, Romano L, et al. Implementation of a dual-phase grating interferometer for multi-scale characterization of building materials by tunable dark-field imaging. SCIENTIFIC REPORTS. 2024;14(1).
IEEE
[1]
C. Organista Castelblanco et al., “Implementation of a dual-phase grating interferometer for multi-scale characterization of building materials by tunable dark-field imaging,” SCIENTIFIC REPORTS, vol. 14, no. 1, 2024.
@article{01HM8YGTZPNR1R9918ACKZ7VEA,
  abstract     = {{The multi-scale characterization of building materials is necessary to understand complex mechanical processes, with the goal of developing new more sustainable materials. To that end, imaging methods are often used in materials science to characterize the microscale. However, these methods compromise the volume of interest to achieve a higher resolution. Dark-field (DF) contrast imaging is being investigated to characterize building materials in length scales smaller than the resolution of the imaging system, allowing a direct comparison of features in the nano-scale range and overcoming the scale limitations of the established characterization methods. This work extends the implementation of a dual-phase X-ray grating interferometer (DP-XGI) for DF imaging in a lab-based setup. The interferometer was developed to operate at two different design energies of 22.0 keV and 40.8 keV and was designed to characterize nanoscale-size features in millimeter-sized material samples. The good performance of the interferometer in the low energy range (LER) is demonstrated by the DF retrieval of natural wood samples. In addition, a high energy range (HER) configuration is proposed, resulting in higher mean visibility and good sensitivity over a wider range of correlation lengths in the nanoscale range. Its potential for the characterization of mineral building materials is illustrated by the DF imaging of a Ketton limestone. Additionally, the capability of the DP-XGI to differentiate features in the nanoscale range is proven with the dark-field of Silica nanoparticles at different correlation lengths of calibrated sizes of 106 nm, 261 nm, and 507 nm.}},
  articleno    = {{384}},
  author       = {{Organista Castelblanco, Caori and Tang, Ruizhi and Shi, Zhitian and Jefimovs, Konstantins and Josell, Daniel and Romano, Lucia and Spindler, Simon and Kibleur, Pierre and Blykers, Benjamin and Stampanoni, Marco and Boone, Matthieu}},
  issn         = {{2045-2322}},
  journal      = {{SCIENTIFIC REPORTS}},
  keywords     = {{Multidisciplinary,RED PINE,RAY,CONTRAST,VISIBILITY,SYSTEMS}},
  language     = {{eng}},
  number       = {{1}},
  pages        = {{14}},
  title        = {{Implementation of a dual-phase grating interferometer for multi-scale characterization of building materials by tunable dark-field imaging}},
  url          = {{http://doi.org/10.1038/s41598-023-50424-6}},
  volume       = {{14}},
  year         = {{2024}},
}

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